HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminobenzoate → HCID 18185339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Reactant | 5-[[(Trifluoromethyl)sulfonyl]amino]-1H-indole-2-carboxylic acid | HCID 18185295 | — |
| Product | HCID 18185339 | HCID 18185339 | — |
Reaction Steps
Same procedure as Example 82 except 5-Trifluoromethansulfonylamino-1H-Indole-2-Carboxylic Acid and 4-aminobenzoic methyl ester was used. 1H-NMR (400 MHz, DMSO-d6) δ 12.74 (s, 1H, COOH), 11.99 (d, J=1.2 Hz, 1H, NHCO), 11.61 (s, 1H, SNH), 10.54 (s, 1H, NH-1), 7.95 (m, 4H, ArH), 7.61 (d, J=2.1 Hz, 1H H-4), 7.50 (m, 2H, H-7 & H-3), 7.14 (dd, J=2, 9 Hz, 1H, H-6), MS m/z 426 (M−H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596772B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-4ddb50555103470da2a62b3a715fe611 |
| Source note | uspto-grants-2003_07 |