HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 2-oxo-1-Pyridin-2-ylmethyl-1,2-dihydro-pyridine-4-carboxylic Acid (4-Methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 2-Methoxy-N-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-isonicotinamide | HCID 10194294 | — |
| Reactant | 2-(2-Bromoethyl)pyridine hydrobromide | HCID 12913859 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-oxo-1-Pyridin-2-ylmethyl-1,2-dihydro-pyridine-4-carboxylic Acid (4-Methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-amide | HCID 10238836 | — |
Reaction Steps
From 2-methoxy-N-(4-methoxy-7-morpholin-4-yl -benzothiazol-2-yl)-isonicotinamide with sodium iodide and 2-(bromoethyl)pyridine hydrobromide in DMF. ES-MS m/e (%): 500 (M+Na+, 30), 478 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599901B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-71e57cc6ccc8474cb7cce89f5a466e67 |
| Source note | uspto-grants-2003_07 |