HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18180103, compound → HCID 17896794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18180103 | HCID 18180103 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 17896794 | HCID 17896794 | 91% |
Reaction Steps
A solution of the cyclopropyl-[4-(2-methoxy-5-nitrophenyl)-piperazin-1-yl]methanone (D17) (1.8 mmol) in ethanol was hydrogenated over 10% Palladium on charcoal catalyst for 2 hrs at room temperature to give the title compound in 91% yield. Found MH+ 276.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599904B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-597062c2af9a4eb495e5b05f406ab81b |
| Source note | uspto-grants-2003_07 |