HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride → HCID 18180134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride | HCID 2735756 | — |
| Reactant | HCID 18180121 | HCID 18180121 | — |
| Product | HCID 18180134 | HCID 18180134 | — |
Reaction Steps
The title compound (E130) was prepared from 4-methoxy-3-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)phenylamine (free base of D39) (100 mg, 0.46 mmol) and 5-chloro-3-methylbenzo[b]thiophene-2-sulfonyl chloride (129 mg, 0.46 mmol) using the method of Example 1 (177 mg, 77%). MH+=463/465.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599904B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-2c9e544f88dc4d3db26089e0d520ee28 |
| Source note | uspto-grants-2003_07 |