HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide diethylacetal → HCID 54176307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Reactant | 7-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one | HCID 14068220 | — |
| Product | HCID 54176307 | HCID 54176307 | — |
Reaction Steps
7-Benzyloxy-3,4-dihydro-2-dimethylaminomethylene-1(2H)naphthalenone was prepared from 7-benzyloxy-3,4-dihydro-1(2H)naphthalenone (6.0 g, 23.8 mmol) and N,N-dimethylformamide diethylacetal (20 ml, 119.4 mmol) to give the desired compound as a pale yellow solid (4.56 g) m.p. 85-86°. MS(ES+) 308 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599908B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-80cec0a8b20c4496b3ec0c5454294acc |
| Source note | uspto-grants-2003_07 |