HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22145275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 129075-84-9 | HCID 251958 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22145275 | HCID 22145275 | — |
Reaction Steps
A mixture of 3-(2-ethylphenyl)propanoic acid (prepared in 3 steps from 1-ethyl-2-iodobenzene, 4.24 g, 23.8 mmole), thionyl chloride (9.50 ml, 130 mmol) and toluene (100 ml) was refluxed for 2 hours. Concentration in vacuo gave 3-(2-ethylphenyl)propanoyl chloride which was taken up in methylene chloride and used in the next step as a crude.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06600015B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-5c1cb8e628a940c689106472e574419d |
| Source note | uspto-grants-2003_07 |