HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69995593, compound → HCID 45115983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69995593 | HCID 69995593 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 45115983 | HCID 45115983 | — |
Reaction Steps
A solution of (R)-2-(cyclopropyl-methyl-carbamoyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (958 mg, 3.57 mmol) in 50% TFA in DCM (5 mL) was stirred at rt for 4 hours. The reaction was concentrated and purified to give (R)-pyrrolidine-2-carboxylic acid cyclopropyl-methyl-amide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599902B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-25da2d766ea14bb89d2f6191a684152c |
| Source note | uspto-grants-2003_07 |