HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 59077731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-formyl-2,4-dimethyl-1H-pyrrole-3-carboxylic Acid | HCID 11073792 | — |
| Reactant | HCID 18180008 | HCID 18180008 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59077731 | HCID 59077731 | — |
Reaction Steps
A mixture of 5-(3,5-dichloro-phenylmethanesulfonyl)-1,3-dihydro-indol-2-one (356 mg, 1 mmol), 5-formyl-2,4-dimethyl-1H-pyrrole-3-carboxylic acid (167 mg) and piperidine (cat. amount) in ethanol was stirred at rt for 2 days. The reaction was concentrated and triturated with HCl (2M solution) to give the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599902B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-30cfd5c7dbec4b618a98e977064d1af5 |
| Source note | uspto-grants-2003_07 |