HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorothymol → HCID 59483417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorothymol | HCID 6982 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 59483417 | HCID 59483417 | — |
Reaction Steps
Following the procedure described for Example 1, Step 1, treatment of a solution (0.174 M) in Et2O of 4-chloro-2-isopropyl-5-methyl-phenol with phosphorus oxychloride (1.0 eq.) and Et3N (1.0 eq.) provided the title compound as a colorless oil. 31P NMR (300 MHz, CD3OD): δ 4.54.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879815B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-2dea10abbb3145fa9230811ce971211c |
| Source note | uspto-grants-2011_02 |