HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 59483408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | L-Alanine, ethyl ester, hydrochloride (1:1) | HCID 2724356 | — |
| Reactant | HCID 59483417 | HCID 59483417 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59483408 | HCID 59483408 | — |
Reaction Steps
Following the procedure described for Example 1, step 2, treatment of a solution in DCM (0.098 M) of 4-chloro-2-isopropyl-5-methylphenyl dichlorophosphate with L-alanine ethyl ester hydrochloride (1.0 eq.) and Et3N (2.0 eq.) provided the title compound as a colorless oil as a 1:1.35* mixture of diastereoisomers. 31P NMR (300 MHz, CD3OD): δ 8.5 and 8.8*.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879815B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-7863db74bba348a29996a1e43f4b2acd |
| Source note | uspto-grants-2011_02 |