HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → N-(1-ethylpropyl)-3,4,5-trifluoroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Ethyl ketone | HCID 7288 | — |
| Reactant | 3,4,5-Trifluoroaniline | HCID 2724991 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | N-(1-ethylpropyl)-3,4,5-trifluoroaniline | HCID 23117858 | — |
Reaction Steps
3-Pentanone, acetic acid and sodium triacetoxyborohydride were added to a 1,2-dichloroethane solution of 3,4,5-trifluoroaniline, for stirring at ambient temperature for 14 hours, to obtain N-(1-ethylpropyl)-3,4,5-trifluoroaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879878B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-c2508dfe0bc74d39a0ce7973d1a6a43f |
| Source note | uspto-grants-2011_02 |