HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 16064296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 16064290 | HCID 16064290 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16064296 | HCID 16064296 | 49.7% |
Reaction Steps
To a solution of 2-[1-(2,6-dichlorophenyl)-2-oxo-2H-quinolizin-6-yl]benzaldehyde (Example 4, 8 mg) in methanol was added sodium borohydride (2 mg) at 0° C. and stirred for ½ hr. The mixture was concentrated and purified by silica gel (methylene chloride/acetone=1/2) to give the title compound (4 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879875B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-303f092237e84b748ff41e59ec0f6848 |
| Source note | uspto-grants-2011_02 |