Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 57700381 | HCID 57700381 | — |
| Product | HCID 16064297 | HCID 16064297 | — |
Reaction Steps
A mixture of 6-chloro-1-(2,6-dichlorophenyl)-2H-quinolizin-2-one (Example 1, 15 mg) in pyrrolidine (0.5 mL) was heated to 90° C. for 2½ hr and then concentrated. The residue was purified by silica gel (methylene chloride/acetone=3/1) to give title compound as a yellow solid (12 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07879875B2 |
|---|
| Source dataset | uspto-grants-2011_02 |
|---|
| ORD ID | ord-f4e692b223df4ce1b51a23d7bfc8d6c9 |
|---|
| Source note | uspto-grants-2011_02 |
|---|
