HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 178506325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 86235795 | HCID 86235795 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 178506325 | HCID 178506325 | — |
Reaction Steps
A solution of 3.8 g (17 mmol) of the crude product of Step A and 4.2 g (22 mmol) of phosphorous pentachloride in 200 mL of dichloroethane was heated at reflux temperature under nitrogen. After 6 h the reaction was cooled to ambient temperature then concentrated in vacuo to yield a crude oil which was carried on to Step C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07884104B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-5e31c15ba87147b68d8838290b414a37 |
| Source note | uspto-grants-2011_02 |