HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59778184, compound → HCID 59983182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59778184 | HCID 59778184 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59983182 | HCID 59983182 | 94.5% |
Reaction Steps
To a solution of 148F (340 mg, 0.69 mmol) in MeOH (8 mL) was added 5% palladium on carbon (200 mg). The resulting suspension was hydrogenated under hydrogen balloon for 1 h., then filtered. The filtrate was concentrated to give title compound (235 mg, 94% yield) as an off-white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07884113B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-6adab01b1eea448abd7c3172f50401b9 |
| Source note | uspto-grants-2011_02 |