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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1363349Generated: October 28, 2026

Acetic Acid → HCID 66933986, compound

https://huagongshe.com/reaction/1363349

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantHCID 66933856HCID 66933856—
SolventMethanolHCID 887—
ProductHCID 66933986HCID 66933986—

Reaction Conditions

Temperature52.5 °C

Reaction Steps

Acetic acid (0.0068 g, 0.11 mmol) was added to the suspension of compound of example 47 (0.05 g, 0.11 mmol) in methanol (2 mL). It was stirred for 5 min. at 50-55° C. to get clear solution. The reaction mixture was concentrated and solid was dried to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07884127B2
Source datasetuspto-grants-2011_02
ORD IDord-e71afc028d7b44e28e58673fcd4249af
Source noteuspto-grants-2011_02