Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 66933856 | HCID 66933856 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66933986 | HCID 66933986 | — |
Reaction Steps
Acetic acid (0.0068 g, 0.11 mmol) was added to the suspension of compound of example 47 (0.05 g, 0.11 mmol) in methanol (2 mL). It was stirred for 5 min. at 50-55° C. to get clear solution. The reaction mixture was concentrated and solid was dried to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07884127B2 |
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| Source dataset | uspto-grants-2011_02 |
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| ORD ID | ord-e71afc028d7b44e28e58673fcd4249af |
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| Source note | uspto-grants-2011_02 |
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