Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1363350Generated: October 29, 2026

Sulfuric Acid → HCID 66933873, compound

https://huagongshe.com/reaction/1363350

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfuric AcidHCID 1118—
ReactantHCID 66933856HCID 66933856—
SolventMethanolHCID 887—
ProductHCID 66933873HCID 66933873—

Reaction Conditions

Temperature52.5 °C

Reaction Steps

H2SO4 solution (55 μL, 5% methanolic solution, 0.055 mmol) was added to the suspension of compound of example 47 (0.025 g, 0.055 mmol) in methanol (2 mL). It was stirred for 5 min at 50-55° C. The reaction mixture was concentrated and solid was dried to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07884127B2
Source datasetuspto-grants-2011_02
ORD IDord-e933ea34ed854311956724b9d5f238bf
Source noteuspto-grants-2011_02