Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 66933856 | HCID 66933856 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66933873 | HCID 66933873 | — |
Reaction Steps
H2SO4 solution (55 μL, 5% methanolic solution, 0.055 mmol) was added to the suspension of compound of example 47 (0.025 g, 0.055 mmol) in methanol (2 mL). It was stirred for 5 min at 50-55° C. The reaction mixture was concentrated and solid was dried to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07884127B2 |
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| Source dataset | uspto-grants-2011_02 |
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| ORD ID | ord-e933ea34ed854311956724b9d5f238bf |
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| Source note | uspto-grants-2011_02 |
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