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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1363351Generated: October 30, 2026

Nitric Acid → HCID 66933957, compound

https://huagongshe.com/reaction/1363351

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNitric AcidHCID 944—
ReactantHCID 66933856HCID 66933856—
SolventMethanolHCID 887—
ProductHCID 66933957HCID 66933957—

Reaction Conditions

Temperature52.5 °C

Reaction Steps

HNO3 solution (55 μL, 6.9% methanolic solution, 0.055 mmol) was added to the suspension of compound of example 47 (0.025 g, 0.055 mmol) in methanol (2 mL). It was stirred for 5 min. at 50-55° C. to get clear solution. The reaction mixture was concentrated and solid was dried to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07884127B2
Source datasetuspto-grants-2011_02
ORD IDord-b64c62d7592c4a09b48bdcd616028cea
Source noteuspto-grants-2011_02