HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-chlorobenzoate → HCID 131728666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-chlorobenzoate | HCID 11895 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 131728665 | HCID 131728665 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131728666 | HCID 131728666 | — |
Reaction Steps
Compound of example 105 (9 g, 29 mmol) in dry DMF (50 mL) was reacted methyl 2-chlorobenzoate (16.5 g, 96.7 mmol) in the presence of NaH (50%, 6.99 g, 145.6 mmol) as described in example 16 to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07884127B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-3fe97e9812e74605bde387897da78036 |
| Source note | uspto-grants-2011_02 |