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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1363373Generated: October 29, 2026

Methyl 2-chlorobenzoate → HCID 131728666, compound

https://huagongshe.com/reaction/1363373

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl 2-chlorobenzoateHCID 11895—
ReactantSodium hydrideHCID 24758—
ReactantHCID 131728665HCID 131728665—
SolventDimethylformamideHCID 6228—
ProductHCID 131728666HCID 131728666—

Reaction Steps

Compound of example 105 (9 g, 29 mmol) in dry DMF (50 mL) was reacted methyl 2-chlorobenzoate (16.5 g, 96.7 mmol) in the presence of NaH (50%, 6.99 g, 145.6 mmol) as described in example 16 to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07884127B2
Source datasetuspto-grants-2011_02
ORD IDord-3fe97e9812e74605bde387897da78036
Source noteuspto-grants-2011_02