Ammonia → HCID 131728667, compound

Participants

Reaction Steps

Compound of example 107 (0.6 g, 1.32 mmol) and triphenylphosphine (0.414 g, 1.58 mmol) were dissolved in THF (10 mL) containing water (0.1 mL). The resultant solution was stirred for 12 h. It was concentrated and the residue obtained was subjected to flash column chromatography using 5% IPA+1% liquor NH3 in CHCl3 as eluant to obtain the title compound.

Provenance & Evidence