HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-[(chlorocarbonyl)oxy]benzoate → HCID 57838898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-[(chlorocarbonyl)oxy]benzoate | HCID 854163 | — |
| Reactant | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| Product | HCID 57838898 | HCID 57838898 | — |
Reaction Steps
4-(methoxycarbonyl)phenyl chloroformate (5.00 g, 23.3 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (4.00 g, 17.9 mmol) according to general procedure 1. Yield=5.54 g, 99%. m/z MH+=302.02. HPLC rt=10.8 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888329B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-2d2949ddcbc74e0ba7b223e2d86bcfb4 |
| Source note | uspto-grants-2011_02 |