Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Product | Methyl (chlorosulfonyl)acetate | HCID 11435213 | — |
Reaction Steps
To chlorosulfonyl chloride (3.34 g, 17.9 mmol) in diethyl ether (30 mL) is added at 0° C. methanol (800 μL, 19.7 mmol). The resulting mixture is stirred at 0° C. during 1 h and the solvent is evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07888351B2 |
|---|
| Source dataset | uspto-grants-2011_02 |
|---|
| ORD ID | ord-9a3b2141b7284048848ae638abe8f55e |
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| Source note | uspto-grants-2011_02 |
|---|
