Hydrochloric Acid → HCID 57779803, compound

Participants

Reaction Steps

A mixture of the product from Step 2 (5.65 g, 15.6 mmol) in tetrahydrofuran (60 mL), methanol (20 mL) and aqueous 1 N lithium hydroxide solution (20 mL) was stirred at room temperature for 18 hours. The mixture was then poured into 0.5 N aqueous HCl solution and extracted with ethyl acetate. The organic extracts were combined, dried over MgSO4, filtered and concentrated in vacuo to give the desired product.

Provenance & Evidence