HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-1-phenylethanone → 3587-84-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-1-phenylethanone | HCID 77698 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3587-84-6 | HCID 572294 | 78.9% |
Reaction Steps
To a stirred solution of 2-methoxy-1-phenylethanone (1.0 g, 6.66 mmol) in ethanol was added sodium borohydride (0.28 g, 7.32 mmol). The reaction mixture was stirred at room temperature for 1 hour. The reaction mixture was quenched with sat. ammonium chloride solution, concentrated. Extracted with ethyl acetate, washed with brine, dried, and concentrated to yield 0.8 g of 2-methoxy-1-phenylethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888366B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-6e2bde9bd215416492fcfa59e9a45d5b |
| Source note | uspto-grants-2011_02 |