Iodoethane → HCID 66919359, compound

HRID 1364505Notes

Reaction equation

HRID 1364505 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:16]3[CH2:15][CH2:14][C:13]([CH2:18][CH:19]([C:21]4[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=4)[OH:20])([CH3:17])[CH2:12][C:11]=3[CH:10]=[N:9]2)=[CH:4][CH:3]=1.I[CH2:28][CH3:29]>>[CH2:28]([O:20][CH:19]([C:21]1[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=1)[CH2:18][C:13]1([CH3:17])[CH2:14][CH2:15][C:16]2[N:8]([C:5]3[CH:6]=[CH:7][C:2]([F:1])=[CH:3][CH:4]=3)[N:9]=[CH:10][C:11]=2[CH2:12]1)[CH3:29]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 66919613HCID 66919613, compound

Product 1

HCID 66919359HCID 66919359, compound

Procedure

Using a procedure analogous to Example 35, the alcohols from Examples 117 and 118 were reacted with iodoethane to give Examples 119 and 120, respectively. MS found: (M+H)+=379.

Workup

  1. customto give Examples 119 and 120

Sources & evidence

ORD record
ord-efc6d34a42d04d779980a34083246d59
Source dataset
uspto-grants-2011_02
Patent number
US07888381B2

Reaction notes

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