HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 66970990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 66971319 | HCID 66971319 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66970990 | HCID 66970990 | 89.9% |
Reaction Steps
To a solution of [3-benzyloxy-1-isopropyl-5-(4-methoxyphenyl)-1H-pyrazol-4-yl]4-methoxy-phenyl methanol (0.11 g) in ethanol (4 mL) was added a catalytic amount of 10% palladium-carbon powder and the mixture was stirred at room temperature under a hydrogen atmosphere overnight. Dichloromethane was added to the mixture and the insoluble material was removed by filtration. The solvent of filtrate was removed under reduced pressure to give the title compound (0.076 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888487B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-b0dfce2a15b74df9b5943e3f50fe9144 |
| Source note | uspto-grants-2011_02 |