Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1365028Generated: October 31, 2026

Dichloromethane → HCID 66970990, compound

https://huagongshe.com/reaction/1365028

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 66971319HCID 66971319—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 66970990HCID 6697099089.9%

Reaction Steps

To a solution of [3-benzyloxy-1-isopropyl-5-(4-methoxyphenyl)-1H-pyrazol-4-yl]4-methoxy-phenyl methanol (0.11 g) in ethanol (4 mL) was added a catalytic amount of 10% palladium-carbon powder and the mixture was stirred at room temperature under a hydrogen atmosphere overnight. Dichloromethane was added to the mixture and the insoluble material was removed by filtration. The solvent of filtrate was removed under reduced pressure to give the title compound (0.076 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07888487B2
Source datasetuspto-grants-2011_02
ORD IDord-b0dfce2a15b74df9b5943e3f50fe9144
Source noteuspto-grants-2011_02