p-Toluenesulfonic acid → HCID 86619059, compound

HRID 1365554Notes

Reaction equation

HRID 1365554 reaction equation
Cl.[NH2:2][CH2:3][C:4](=[O:17])[CH2:5][CH2:6][C:7]([O:9][CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[O:8].C1(C)C=CC([S:24]([OH:27])(=[O:26])=[O:25])=CC=1>>[C:11]1([CH3:10])[C:16]([S:24]([OH:27])(=[O:26])=[O:25])=[CH:15][CH:14]=[CH:13][CH:12]=1.[NH2:2][CH2:3][C:4](=[O:17])[CH2:5][CH2:6][C:7]([O:9][CH2:10][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)=[O:8]

Participants

3

Reactant 2

HCID 6101p-Toluenesulfonic acidHCID 22253144Benzyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1)

Product 1

HCID 86619059HCID 86619059, compound

Procedure

Prepared from benzyl 5-amino-4-oxopentanoate hydrochloride and p-toluenesulfonic acid using the ion-exchange method, mp 120-125° C.

Sources & evidence

ORD record
ord-8008b5d218b7467baa24702c48d41534
Source dataset
uspto-grants-2011_02
Patent number
US07888526B2

Reaction notes

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