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HRID1366864

反应详情

EQUATION

反应方程式

HRID 1366864 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1ccc(C(F)(F)F)cc1Cl
HCID2736675

2-Chloro-4-(trifluoromethyl)benzenesulfonyl chloride

C7H3Cl2F3O2S

结构：Cc1cc(Sc2ccc(S(=O)(=O)N3CCCCC3)cc2)nnc1N
HCID66971400

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Sc2ccc(S(=O)(=O)N3CCCCC3)cc2)nnc1NS(=O)(=O)c1ccc(C(F)(F)F)cc1Cl
HCID57718224

未命名化合物

PROCEDURE

实验过程

Can be prepared from 4-methyl-6-[4-(piperidine-1-sulfonyl) -phenylsulfanyl]-pyridazin-3-ylamine and 2-chloro-4-trifluoromethylbenzenesulfonyl chloride. 1H NMR (CDCl3) 8.30 (1H, d) 7.75 (2H, m) 7.70(1H, s) 7.6(3H, m) 7.05(1H, s) 3.0 (4H, m) 2.1 (3H, s) 1.6(4H, m) 1.40(2H, m) LCMS Polarity/Scan type: Negative Q1 Scan. M.wt. 605 (—H), 607 (—H). Retention time 7.39 minutes. HPLC MS8 Retention time 5.36 minutes.