HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-(trifluoromethyl)benzenethiol → HCID 66918793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-(trifluoromethyl)benzenethiol | HCID 50997997 | — |
| Reactant | HCID 86649032 | HCID 86649032 | — |
| Product | HCID 66918793 | HCID 66918793 | — |
Reaction Steps
The title compound was prepared in analogy to example 68 step 8 using (1R,2R)-4-methanesulfonyloxy-2-trityloxymethyl-cyclopentanecarboxylic acid ethyl ester (epimeric mixture, example 152 step 3) and 4-bromo-2-trifluoromethyl-benzenethiol (example 58, intermediate 1). Colorless oil (43%). MS (EI): 691.0 (M+Na)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893099B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-f6499520ac154a78b13921f9b32840a6 |
| Source note | uspto-grants-2011_02 |