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HRID1367894

反应详情

EQUATION

反应方程式

HRID 1367894 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2cnc(C(=O)O)cc2c1
HCID57306949

未命名化合物

结构：CC(C)(C)OC(=O)C1(C(=O)O)NCCc2ccc(O)cc21
HCID66940410

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2cc(C(=O)O)ncc2c1
HCID10822014

未命名化合物

收率 17%

PROCEDURE

实验过程

0.25 g (17% in 4 steps) 7-methoxy-isoquinoline-3-carboxylic acid was prepared according to procedure described for the synthesis of 6-methoxy-isoquinoline-3-carboxylic acid (in Example 294) starting from 2.0 g (6.8 mmol) of boc-7-hydroxy-tetrahydroisoquinoline carboxylic acid using 179 mg (0.824 mmol). LCMS: 204 (M+1)+.