HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 69831977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 12071996 | HCID 12071996 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69831977 | HCID 69831977 | 86% |
Reaction Steps
To a ethanol solution of 9.32 g of (±)-3-[(S)-3-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-2-carbonyl)piperidino]-N-(3,4-methylenedioxyphenyl)propanamide was added 2.07 g of fumaric acid, and the mixture was evaporated in vacuo. Thus, 9.38 g of (±)-3-[(S)-3-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-2-carbonyl)piperidino]-N-(3,4-methylenedioxyphenyl)propanamide fumarate was obtained as colorless crystals from ethanol/2-butanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573279B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-02bd1b6e0ce44f0597e392876023d011 |
| Source note | uspto-grants-2003_06 |