HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 135697913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-(4-Methoxyphenyl)ethanimidamide hydrochloride | HCID 12203394 | — |
| Reactant | Ethyl 3-acetamido-2-oxobutanoate | HCID 22245807 | — |
| Product | HCID 135697913 | HCID 135697913 | — |
Reaction Steps
Analogously to Example 10A, 5.1 g (25.4 mmol) of 2-(4-methoxyphenyl)ethanamidine hydrochloride are reacted with 1.53 g (30.5 mmol) of hydrazine hydrate and 7.14 g (38.1 mmol) of ethyl 3-(acetylamino)-2-oxobutanoate to give N-{1-[3-(4-methoxybenzyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]ethyl}acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573263B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-c5164692c10a43078eb064d0de47a043 |
| Source note | uspto-grants-2003_06 |