HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 135824715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 18519815 | HCID 18519815 | — |
| Reactant | Ethyl 3-acetamido-2-oxobutanoate | HCID 22245807 | — |
| Product | HCID 135824715 | HCID 135824715 | — |
Reaction Steps
Analogously to Example 10A, 3.5 g (15.8 mmol) 2-(6-quinolinyl)ethanamidine hydrochloride are reacted with 950 mg (19.0 mmol) of hydrazine hydrate and 4.43 g (23.7 mmol) of ethyl 3-(acetylamino)-2-oxobutanoate to give N-{1-[5-oxo-3-(6-quinolinylmethyl)-4,5-dihydro-1,2,4-triazin-6-yl]ethyl}acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573263B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-3d7ddad725e241d1a3532bf3bd2b6371 |
| Source note | uspto-grants-2003_06 |