HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18520269, compound → HCID 18520275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18520269 | HCID 18520269 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18520275 | HCID 18520275 | — |
Reaction Steps
4N Hydrochloric acid/ethyl acetate solution (0.50 ml) was added to a solution containing N-[3-(dimethylamino)propyl]-3-[2-(octadecyloxy)phenyl]propanamide (0.42 g) in ethyl acetate (4 ml) at room temperature. After being stirred for 10 minutes, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-ethanol, thereby yielding the entitled compound (0.30 g) as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573297B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-352680923de9419c87131e79887d8282 |
| Source note | uspto-grants-2003_06 |