Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-[2-(4-Methylpiperazino)-2-oxoethyl]phenyl N-octadecylcarbamate → HCID 18520252, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-[2-(4-Methylpiperazino)-2-oxoethyl]phenyl N-octadecylcarbamate | HCID 18520253 | — |
| 반응물 | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 18520252 | HCID 18520252 | — |
반응 단계
4N Hydrochloric acid/ethyl acetate solution (1.40 ml) was added to a solution containing 2-[2-(4-methylpiperazino)-2-oxoethyl]phenyl N-octadecylcarbamate (2.50 g) in ethyl acetate (25 ml) at room temperature. After being stirred for 30 minutes, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-ethanol, thereby yielding the entitled compound (2.52 g) as white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06573297B2 |
| 출처 데이터셋 | uspto-grants-2003_06 |
| ORD ID | ord-361ecb7a0c8b4b3d982365cd87b73bac |
| 출처 메모 | uspto-grants-2003_06 |