HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromobenzene → HCID 178487486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromobenzene | HCID 7961 | — |
| Reactant | (6-Methoxynaphthalen-2-yl)-(1-trityl-1H-imidazol-4-yl)ketone | HCID 11733735 | — |
| Product | HCID 178487486 | HCID 178487486 | — |
Reaction Steps
In a similar manner to that described in Example 6-(i), the reaction of bromo benzene (0.85 ml) with (6-methoxynaphthalen-2-yl)-(1-trityl-1H-imidazol-4-yl)ketone (1.0 g) was carried out. The reaction mixture was purified by silica gel column chromatography (eluent, hexane:ethyl acetate=3:1→2:1) to give the titled compound (0.98 g) as a pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573289B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-af224a6b71004f0d835c8be01c8007e6 |
| Source note | uspto-grants-2003_06 |