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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1368517Generated: November 1, 2026

Bromobenzene → HCID 178487486, compound

https://huagongshe.com/reaction/1368517

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromobenzeneHCID 7961—
Reactant(6-Methoxynaphthalen-2-yl)-(1-trityl-1H-imidazol-4-yl)ketoneHCID 11733735—
ProductHCID 178487486HCID 178487486—

Reaction Steps

In a similar manner to that described in Example 6-(i), the reaction of bromo benzene (0.85 ml) with (6-methoxynaphthalen-2-yl)-(1-trityl-1H-imidazol-4-yl)ketone (1.0 g) was carried out. The reaction mixture was purified by silica gel column chromatography (eluent, hexane:ethyl acetate=3:1→2:1) to give the titled compound (0.98 g) as a pale yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06573289B1
Source datasetuspto-grants-2003_06
ORD IDord-af224a6b71004f0d835c8be01c8007e6
Source noteuspto-grants-2003_06