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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1368562Generated: October 31, 2026

HCID 22018460, compound → HCID 22018435, compound

https://huagongshe.com/reaction/1368562

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22018460HCID 22018460—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
ProductHCID 22018435HCID 2201843586.1%

Reaction Steps

(6-methoxynaphthalen-2-yl)(thiazol-5-yl)methanol (2.0 g) was dissolved in dichloromethane (30 ml). To the solution was added manganese dioxide (6.0 g), and the mixture was stirred at room temperature for 3 h. The mixture was filtered with celite and the cake was rinsed with dichloromethane. The filtrate was concentrated and the obtained residue was recrystallized from ethyl acetate to give the titled compound (1.71 g) as a pale yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06573289B1
Source datasetuspto-grants-2003_06
ORD IDord-862ad7b7582c4f55b47c009936194fb9
Source noteuspto-grants-2003_06