HCID 18520707, compound → HCID 59069781, compound
Reaction equation
[C:1]([C:4]1[C:8]([Br:9])=[C:7]([CH3:10])[S:6][C:5]=1[CH3:11])(=[O:3])[CH3:2]>O1CCCC1>[CH3:11][C:5]1[S:6][C:7]([CH3:10])=[C:8]([Br:9])[C:4]=1[C@H:1]([OH:3])[CH3:2]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
3-Acetyl-4-bromo-2,5-dimethylthiophene (78.5 mmol) was reduced by means of Ipc2BCl in tetrahydrofuran using the general method of Brown et al. (J. Org. Chem. 1989, 54, 4504).
Sources & evidence
- ORD record
- ord-b27e134446b546e8aeff9851882d8885
- Source dataset
- uspto-grants-2003_06
- Patent number
- US06573389B1
Reaction notes
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