Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 11300612 | HCID 11300612 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18520435 | HCID 18520435 | — |
Reaction Steps
A 1.43 g (5.01 mmol) portion of 2,4-dichloro-6-(4-methoxybenzylamino)-1,3,5-triazine was suspended in 100 ml of ethanol, mixed with 303 μl (5.01 mmol) of 2-aminoethanol and 693 mg of potassium carbonate and stirred at 45° C. for 1 day. After evaporation of the solvent under a reduced pressure, water was added to the residue and the resulting precipitate was collected by filtration to obtain 1.56 g (quantitative) of the title compound as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06573377B1 |
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| Source dataset | uspto-grants-2003_06 |
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| ORD ID | ord-90dc0f7fb4634e79820c0c7d0f4da809 |
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| Source note | uspto-grants-2003_06 |
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