Ethanol → HCID 18520417, compound

Participants

Reaction Steps

After suspending 7.79 g portion of 2-amino-4-chloro-6-hydrazinopyrimidine in 100 ml of ethanol, 10.7 g of methyl methoxymethylenepropionylacetate was added thereto, and the mixture was stirred at room temperature for 20 minutes and then at 80° C. for 3 hours. After allowing the reaction solution to stand at 0° C. for 48 hours, the resulting precipitate was collected by filtration and dried to obtain 12.88 g of the title compound.

Provenance & Evidence