HCID 6993440, compound → HCID 100979516, compound

Participants

Reaction Steps

Z-L-Ala-L-Ala-NH2 (12) (Katakai et al., Macromolecules, 6:827-831 (1973), which is hereby incorporated by reference): 1H NMR (DMSO-d6) δ1.20 (2×d, J=7 Hz, 6H, 2×CH3), 4.10, 4.20 (m, 2H, 2×NHCHCO), 5.00 (s, 2H, OCH2Ph), 7.20-7.40 (m, 5H, Ph); 13C NMR (DMSO-d6) δ18.1, 18.4, 47.9, 50.1, 65.4, 127.7, 128.4, 137.0, 155.8, 172.0. 174.1. HRMS (FAB+) MH+ calcd 294.1454 found 294.1457. [α]25D=−20.4 (c 0.77, MeOH).

Provenance & Evidence