HuagongsheHuagongshe Chemistry Print Report · For research reference only
2H-Pyran, tetrahydro-2-(2-iodoethoxy)- → HCID 86590392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2H-Pyran, tetrahydro-2-(2-iodoethoxy)- | HCID 11118662 | — |
| Reactant | HCID 69544513 | HCID 69544513 | — |
| Product | HCID 86590392 | HCID 86590392 | — |
Reaction Steps
2-(2-Chlorophenyl-1-[4-(2-piperidinylethoxy)phenyl]-4-(tetrahydropyranyloxy)butan-1-one is prepared by PTC reaction according to the method described in the example 4d using 2-(2-chlorophenyl)-1-[4-(2-piperidinylethoxy)phenyl]ethanone (1.5 g, 4.2 mmol) and 2-tetrahydropyranyloxy-1-iodoethane (1.3 g, 5.1 mmol) as the starting materials. The product (1.6 g) is used for the following reaction step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06576645B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-d591a31d519147859c1f013c4935cb1d |
| Source note | uspto-grants-2003_06 |