HRID1368947

反应详情

EQUATION

反应方程式

HRID 1368947 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

4-Nitrobenzophenone (5.0 g, 0.022 mol) is dissolved in ethanol-dichloromethane (40 ml:30 ml) and hydrogenated at room temperature with 10% palladium on carbon (0.5 g) as a catalyst. The catalyst is filtered off and the filtrate is evaporated to dryness. The product is used in the next reaction step without further purification. Yield 5.2 g.

WORKUP

后处理

  1. filtrationThe catalyst is filtered off
  2. customthe filtrate is evaporated to dryness
  3. customThe product is used in the next reaction step without further purification