HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanone, (4-nitrophenyl)phenyl- → 4-Aminobenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanone, (4-nitrophenyl)phenyl- | HCID 70839 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | 4-Aminobenzophenone | HCID 14346 | — |
Reaction Steps
4-Nitrobenzophenone (5.0 g, 0.022 mol) is dissolved in ethanol-dichloromethane (40 ml:30 ml) and hydrogenated at room temperature with 10% palladium on carbon (0.5 g) as a catalyst. The catalyst is filtered off and the filtrate is evaporated to dryness. The product is used in the next reaction step without further purification. Yield 5.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06576645B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-6739355601ed42fb8d669827d530fd96 |
| Source note | uspto-grants-2003_06 |