HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23567163, compound → HCID 23567164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23567163 | HCID 23567163 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 23567164 | HCID 23567164 | — |
Reaction Steps
The sub-title compound was prepared according to the method described in Example 1(iv) above from 7-methoxy-3,4-dihydronaphthalen-1-yl-carboxylic acid, methyl ester (3.3 g; 15 mmol; see Example 9(i) above) and Pd/C (10%; 0.5 g). The resultant mixture was filtered through Hyflo and concentrated. The crude product was purified using flash chromatography (Si-gel; heptane:EtOAc; 4:1). Yield 2.4 g (72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06576657B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-ceed51625d774a7a8d7aeb74e7cc891e |
| Source note | uspto-grants-2003_06 |