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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1369002Generated: October 29, 2026

HCID 23567163, compound → HCID 23567164, compound

https://huagongshe.com/reaction/1369002

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23567163HCID 23567163—
CatalystPalladiumHCID 23938—
ProductHCID 23567164HCID 23567164—

Reaction Steps

The sub-title compound was prepared according to the method described in Example 1(iv) above from 7-methoxy-3,4-dihydronaphthalen-1-yl-carboxylic acid, methyl ester (3.3 g; 15 mmol; see Example 9(i) above) and Pd/C (10%; 0.5 g). The resultant mixture was filtered through Hyflo and concentrated. The crude product was purified using flash chromatography (Si-gel; heptane:EtOAc; 4:1). Yield 2.4 g (72%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06576657B2
Source datasetuspto-grants-2003_06
ORD IDord-ceed51625d774a7a8d7aeb74e7cc891e
Source noteuspto-grants-2003_06