Hydrochloric Acid → HCID 178460452, compound

Participants

Reaction Steps

A mixture of 100 mmol of 4a-(1-acryloyloxy-1-methylethyl)-8a-(2-methoxyethoxymethoxy)-cis-decalin, 6 N-hydrochloric acid (150 mmol in terms of HCl), and 30 ml of acetone was stirred at room temperature for 1 hour. The resulting reaction mixture was concentrated to yield 4a-(1-acryloyloxy-1-methylethyl)-8a-hydroxy-cis-decalin represented by the following formula (yield: 98%). The conversion rate from 4a-(1-acryloyloxy-1-methylethyl)-8a-(2-methoxyethoxymethoxy)-cis-decalin was 99%.

Provenance & Evidence