HRID13692

反应详情

EQUATION

反应方程式

HRID 13692 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Dissolve 7-nitroindole in ethanol and add ammonium formate (10 equivalents) and a catalytic amount of 10% palladium on carbon. Heat the mixture to reflux for 1 hr before cooling, filter through celite, and evaporate to provide the product as a purple solid (99%).

WORKUP

后处理

  1. temperatureHeat the mixture
  2. temperatureto reflux for 1 hr
  3. temperaturebefore cooling
  4. filtrationfilter through celite
  5. customevaporate