HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11403711, compound → HCID 53773271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11403711 | HCID 11403711 | — |
| Reactant | HCID 12071476 | HCID 12071476 | — |
| Reactant | HCID 178526251 | HCID 178526251 | — |
| Product | HCID 53773271 | HCID 53773271 | — |
Reaction Steps
According to the procedure of Example 6 (a), except substituting 6-(methylamino)-2-pyridylethanol for the 2-[(3-hydroxy-1-propyl)amino]pyridine-N-oxide, and ethyl (S)-10,11-dihydro-3-hydroxy-5H-dibenzo[a,d]cycloheptene-10-acetate for ethyl (R)-10,11-dihydro-3-hydroxy-5H-dibenzo[a,d]cycloheptene-10-acetate, the title compound was obtained as colorless oil following silica gel chromatography (0.2-2% MeOH/CH2Cl2): MS (ES) 431.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06576643B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-1d4065fec53d49b588cf5e3d41ae7524 |
| Source note | uspto-grants-2003_06 |