Trifluoroacetic acid → HCID 18518384, compound

Participants

Reaction Steps

According to the procedure of Example 6 (c), except substituting ethyl (±)-10,11-dihydro-3-[3-(isoquinoline-1-ylamino)-1-propyloxy]-5H-dibenzo[a,d]cycloheptene-10-acetate for the ethyl (R)-10,11-dihydro-3-[3-(pyridin-2-ylamino)-1-propyloxy]-5H-dibenzo[a,d]cycloheptene-10-acetate, the title compound was prepared as an amber solid: MS (ES) m/e 453.2(M+H)+. Anal. Calcd for C29H28N2O3.1.3 TFA.0.25 H2O: C, 62.71; H, 4.96; N, 4.63. Found: C, 62.45; H, 4.92; N, 4.41.

Provenance & Evidence