2-Mercaptoethanol → HCID 18508433, compound

HRID 1369320Notes

Reaction equation

HRID 1369320 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:21])[C:9]2[CH:14]=[CH:13][C:12]([O:15][CH2:16][CH2:17][CH2:18][CH3:19])=[CH:11][C:10]=2[OH:20])=[CH:4][CH:3]=1.[SH:22][CH2:23][CH2:24][OH:25].C(=O)([O-])[O-].[K+].[K+]>>[CH2:16]([O:15][C:12]1[CH:13]=[CH:14][C:9]([C:8]([C:5]2[CH:6]=[CH:7][C:2]([S:22][CH2:23][CH2:24][OH:25])=[CH:3][CH:4]=2)=[O:21])=[C:10]([OH:20])[CH:11]=1)[CH2:17][CH2:18][CH3:19]

Participants

4

Reactant 3

HCID 15672-MercaptoethanolHCID 11430Potassium CarbonateHCID 18508436HCID 18508436, compound

Product 1

HCID 18508433HCID 18508433, compound

Procedure

Following the procedure of Example 2, the title compound is prepared by reacting equimolar amounts of 4′-chloro-2-hydroxy-4-butoxybenzophenone and 2-mercaptoethanol in the presence of potassium carbonate.

Sources & evidence

ORD record
ord-80cb1bfcc62747d2af4eea891e2a1aec
Source dataset
uspto-grants-2003_06
Patent number
US06576797B1

Reaction notes

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